Abstract: This study investigated the distribution and the current situation of VOCS emissions of rubber and plastic products industry in Dalian, and carried out VOCS component spectrum monitoring and analysis for typical enterprises. In terms of treatment technology research, the advantages and disadvantages of VOCs treatment technology in rubber and plastic products industry were compared, and on the basis of analyzing the polluting components and pollution characteristics of VOCs, reasonable treatment technology application was selected to control VOCs exhaust gas in a large tire factory, and remarkable results have been achieved.